Neck growth kinetics during polymer sintering for powder-based processes

Densification Kinetics and Structural Evolution During Microwave and Pressureless Sintering of 15 nm Titanium Nitride Powder

Microwave sintering (MWS) of commercially available 15-nm-size nanocrystalline TiN powder was studied. Densification kinetics and grain growth mechanisms of nano-TiN were evaluated using non-isothermal heating up to 1500 °C with variable heating rates. A true nanocrystalline ceramic with ~80-nm-size grains and 94.5 % theoretical density was obtained via MWS consolidation at 1400 °C. At higher t...

Lubricant Pyrolysis During Sintering of Powder Metallurgy Compacts

The chemistry surrounding the pyrolysis of N,NЈ-ethylenebisstearimide (EBS) compacted with iron powder is described for the first time. Heat treatment is carried out in a 5 vol pct hydrogen atmosphere (balance nitrogen) over the 100 °C to 850 °C range. The exhaust from the furnace is monitored by Fourier transform infrared and dispersive ultraviolet absorption spectroscopy; condensable material...

Improving Accuracy of Powder Sintering-based SFF Processes by Metal Deposition from Nanoparticle Dispersion

Solid Freeform Fabrication processes such as three-dimensional printing (3DP) and selective laser sintering (SLS) produce porous parts that must be densified. New steel infiltration methods can produce parts of standard alloy compositions with properties comparable to wrought materials. However, the infiltration process introduces dimensional errors due to both shrinkage and creep—particularly ...

Nano Powder Direct Metal Sintering Systems Specification

Post Treatment Process and Selective Laser Sintering Mechanism of Polymer-Coated Mo Powder

A novel preparing method of polymer-coated molybdenum powder was presented. A type of multi-component polymer-coated molybdenum powder was chosen for selective laser sintering. The effect of the process parameters on the part’s characteristics is investigated. Based on our study for dynamic laser sintering process of polymer-coated molybdenum powder, its laser sintering mechanism was reported a...